- CAS
- Purity
- 2981-10-4
- 99%
Location：Home > Pharmaceutical
Reputable manufacturer supply 1-(1-Piperidino)cyclohexene 2981-10-4 in stock with high standard
- Molecular Formula: C11H19 N
- Molecular Weight: 165.279
- Appearance/Colour: Clear yellow liquid
- Vapor Pressure: 0.011mmHg at 25°C
- Refractive Index: 1.5140
- Boiling Point: 262.2oCat760mmHg
- PKA: 8.88±0.20(Predicted)
- Flash Point: 102.8oC
- PSA： 3.24000
- Density: 0.978g/cm3
- LogP: 2.86810
1-(1-Piperidino)cyclohexene(Cas 2981-10-4) Usage
InChI:InChI=1/C11H19N/c1-3-7-11(8-4-1)12-9-5-2-6-10-12/h7H,1-6,8-10H2
2981-10-4 Relevant articles
A general and efficient method for the synthesis of 9-trifluoromethylated [1,2,4]triazolo[1,5-a]azepine derivatives
Ding, Zongbiao,Xia, Shijing,Ji, Xiaojun,Yang, Haiyan,Tao, Fenggang,Wang, Quanrui
, p. 349 - 354 (2002)
(1-Chloro-2-trifluoromethylcyclohexyl)az...
Pyridone derivative and application thereof in preparation of medicine for preventing and/or treating tuberculosis caused by Mycobacterium tuberculosis
-
Paragraph 0085-0089, (2021/07/01)
The invention provides a pyridone deriva...
1 microwave-induced montmorillonite-mediated facile synthesis of enamines
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, p. 249 - 254 (2020/01/08)
Montmorillonite clay-mediated simple and...
Synthesis and Cytotoxic Evaluation of Novel 1,2,3-Triazole-4-Linked (2E,6E)-2-Benzylidene-6-(4-nitrobenzylidene)cyclohexanones
Mahdavi, Mohammad,Akhbari, Maryam,Saeedi, Mina,Karimi, Maryam,Foroughi, Niloufar,Karimpour-Razkenari, Elahe,Alinezhad, Heshmatollah,Foroumadi, Alireza,Shafiee, Abbas,Akbarzadeh, Tahmineh
, p. 175 - 180 (2016/04/19)
This work describes the synthesis of nov...
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Paragraph 0058, (2017/01/02)
PROBLEM TO BE SOLVED: To provide especia...
2981-10-4 Process route
-
-
110-89-4
piperidine
-
-
108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone
-
-
2981-10-4
1-(cyclohex-1-en-1-yl)piperidine
Conditions
| Conditions | Yield |
|---|---|
|
With
Montmorillonite K 10 clay;
for 0.133333h;
microwave (160 Watts) irradiation;
|
95%
|
|
Envirocat EPZG;
for 0.0333333h;
Irradiation;
|
90%
|
|
With
K-10 Montmorillonite clay;
In
toluene;
for 3h;
Heating;
|
86%
|
|
In
benzene;
Heating;
|
85%
|
|
piperidine; cyclohexanone;
In
pentane;
at 20 ℃;
for 1h;
With
titanium tetrachloride;
In
pentane;
at 0 - 20 ℃;
for 6h;
|
84.2%
|
|
piperidine; cyclohexanone;
In
pentane;
at 20 ℃;
for 1h;
Inert atmosphere;
With
titanium tetrachloride;
In
pentane;
at 0 - 20 ℃;
for 6.5h;
Inert atmosphere;
|
84.2%
|
|
With
bis-(trimethylsilyl)acetamide; methyl iodide;
In
Petroleum ether;
at 35 - 45 ℃;
for 3.5h;
|
80%
|
|
With
montmorillonite K10 Clay;
at 50 ℃;
for 0.0333333h;
Microwave irradiation;
|
80%
|
|
With
toluene-4-sulfonic acid;
In
benzene;
Heating;
|
78%
|
|
for 4h;
|
68%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 109 - 123 ℃;
for 59h;
Large scale;
|
65.2%
|
|
In
benzene;
for 12h;
Heating;
|
50%
|
|
With
calcium oxide;
2-taegiges Erwaermen; Erhitzen des Reaktionsprodukts unter vermindertem Druck.;
|
|
|
With
benzene;
Entfernen des entstehenden Wassers.;
|
|
|
|
|
|
In
benzene;
|
|
|
With
sulfuric acid;
In
benzene;
Yield given;
Heating;
H2O was collected as the benzene azeotrope;
|
|
|
With
4 A molecular sieve; toluene-4-sulfonic acid;
In
toluene;
for 21h;
Heating;
|
|
|
With
toluene-4-sulfonic acid;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 6h;
Reflux;
|
|
|
Acidic conditions;
|
|
|
In
toluene;
for 8h;
Reflux;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 120 ℃;
|
-
-
110-89-4
piperidine
-
-
110-83-8
cyclohexene
-
-
2981-10-4
1-(cyclohex-1-en-1-yl)piperidine
Conditions
| Conditions | Yield |
|---|---|
|
With
toluene-4-sulfonic acid;
In
benzene;
|
2981-10-4 Upstream products
-
110-89-4
piperidine
-
108-94-1
cyclohexanone
-
4442-11-9
lithium piperidide
-
110-83-8
cyclohexene
2981-10-4 Downstream products
-
2625-30-1
nitromethylcyclohexane
-
2591-86-8
N-Formylpiperidine
-
4594-78-9
cyclohexanone-2-propionitrile
-
6407-39-2
N-cyclohexylidenebutylamine